A Simple Protein Purification and Folding Experiment for General Chemistry Laboratory

Document Type

Article

Publication Date

11-1-2000

Journal / Book Title

Journal of Chemical Education

Abstract

Most general chemistry laboratories contain a surfeit of inorganic chemistry and little or no biochemistry. We describe a simple procedure for the crude purification of a chromoprotein suitable for a general chemistry laboratory. The protein, phycocyanin, is easy to purify and very stable. It contains a chromophore that can serve to report the integrity of the protein structure: the chromoprotein is dark blue when the protein is folded in its native conformation, and it turns a very pale blue when the protein is unfolded or denatured. The students must identify intermolecular forces present in the co-solvents added and determine their effect on the protein structure. The simplicity of the protein purification procedure will allow phycocyanin to be readily adopted in the general chemistry laboratory.

DOI

10.1021/ed077p1456

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